GSK-1070916_RP-HPLC_13727_MedChemExpress

=====================================================================Acq. Operator : WRH(HPLC-09) Seq. Line : 6Acq. Instrument : Instrument 1 Location : Vial 1Injection Date : 4/14/2017 11:11:11 AM Inj : 1 Inj Volume : 5.000 µlAcq. Method : D:\\CHEM32\\DATA\\20170414\\20170414 2017-04-14 08-49-53\\10-80A,15MIN,210NM,BC. MLast changed : 10/10/2016 9:45:08 AM by LCY(HPLC-09)Analysis Method : D:\\CHEM32\\METHODS\\RP-HPLC\\10-80,15MIN,210NM,AD.MLast changed : 4/13/2017 4:38:46 PM by WRH(HPLC-09) (modified after loading)Catalog No : HY-70044 Batch#13727 BK A-RP-199 Additional Info : Peak(s) manually integrated VWD1 A, Wavelength=210 nm (D:\\CHEM32\\DATA\\20170414\\20170414 2017-04-14 08-49-53\\001-0601.D)mAU100500-50-10005101520min

===================================================================== Area Percent Report =====================================================================

Sorted By : Signal

Multiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs

No peaks found

===================================================================== *** End of Report ***

Instrument 1 4/14/2017 12:48:42 PM WRH(HPLC-09)Page 1 of 1

Data File D:\\CHEM32\\DATA\\20170414\\20170414 2017-04-14 08-49-53\\037-0701.DSample Name: CPK2017-413-13727

=====================================================================Acq. Operator : WRH(HPLC-09) Seq. Line : 7Acq. Instrument : Instrument 1 Location : Vial 37Injection Date : 4/14/2017 11:35:39 AM Inj : 1 Inj Volume : 5.000 µlAcq. Method : D:\\CHEM32\\DATA\\20170414\\20170414 2017-04-14 08-49-53\\10-80A,15MIN,210NM,BC. MLast changed : 10/10/2016 9:45:08 AM by LCY(HPLC-09)Analysis Method : D:\\CHEM32\\METHODS\\RP-HPLC\\10-80,15MIN,210NM,AD.MLast changed : 4/13/2017 4:38:46 PM by WRH(HPLC-09) (modified after loading)Catalog No : HY-70044 Batch#13727 A-RP-199 Additional Info : Peak(s) manually integrated VWD1 A, Wavelength=210 nm (D:\\CHEM32\\DATA\\20170414\\20170414 2017-04-14 08-49-53\\037-0701.D) 7.100mAU200015001000 5.931 66..452505 6.882 7.348 7.647 7.957 8.267 5.141 89..808177 9.36350000 10.340 10.5875101520min

===================================================================== Area Percent Report =====================================================================

Sorted By : Signal

Multiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs

Signal 1: VWD1 A, Wavelength=210 nm

Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %

----|-------|----|-------|----------|----------|--------| 1 5.141 MM 0.0654 11.38878 2.90428 0.1033 2 5.931 MM 0.0610 59.96109 16.37810 0.5440 3 6.420 MM 0.0579 5.08954 1.46564 0.0462 4 6.555 MM 0.0570 15.14627 4.42730 0.1374 5 6.882 MM 0.0527 5.49407 1.73836 0.0498 6 7.100 MF 0.0762 1.08217e4 2368.01392 98.1749 7 7.348 FM 0.0674 19.58509 4.84293 0.1777 8 7.647 MM 0.0650 13.62726 3.49331 0.1236 9 7.957 MM 0.0729 7.84350 1.79268 0.0712 10 8.267 MM 0.0696 8.94263 2.13991 0.0811 11 8.887 MF 0.0810 14.76468 3.03799 0.1339 12 9.017 FM 0.0881 7.60051 1.43841 0.0690 13 9.363 MM 0.0805 14.24489 2.94997 0.1292Instrument 1 4/14/2017 12:48:14 PM WRH(HPLC-09)

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Data File D:\\CHEM32\\DATA\\20170414\\20170414 2017-04-14 08-49-53\\037-0701.DSample Name: CPK2017-413-13727

Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %

----|-------|----|-------|----------|----------|--------| 14 10.340 MM 0.0729 9.31310 2.12846 0.0845 15 10.587 MM 0.0687 8.17325 1.98345 0.0741

Totals : 1.10229e4 2418.73471

===================================================================== *** End of Report ***

Instrument 1 4/14/2017 12:48:14 PM WRH(HPLC-09)Page 2 of 2